To compression-mould Bakelite, weigh a charge of moulding powder equal to the part volume times the material density times 1.05, load it into a steel mould preheated to 160-180 degrees Celsius, close the press at 10-30 MPa and hold for 1-5 minutes per millimetre of thickness. The press force is the pressure times the part’s projected area, which for an 80 mm by 50 mm part is 40-120 kN.
Part of Plastics and Polymers
Compression molding of thermosets is the pressing of a measured charge of powder in a heated steel mold so that it flows, fills the cavity and cures into a rigid part.
What You Need
- A two-part steel mold machined to the final shape, with draft and rounded corners: Mold Design.
- A press that develops the force: a hydraulic press (Hydraulic Press) or a screw press (Screw Mechanisms).
- A way to heat the mold to 160-180 °C and measure it. The manufacturing carrier gives 150-180 °C. The scratch carrier’s 160-180 °C range is the one written for hexa-containing powder.
- Moulding powder from Synthesis and Molding, weighed on a scale.
Method: The Carrier’s Six Steps
Step 1: Calculate the charge. Charge weight = part volume × material density × 1.05. The 1.05 overfills slightly so that the cavity fills and a thin flash escapes.
Step 2: Preheat the mold in an oven.
Step 3: Load the charge and close the mold in the press.
Step 4: Apply heat and pressure per the material requirements: 10-30 MPa.
Step 5: Hold for the cure time. The scratch carrier gives 1-5 minutes per millimetre of thickness. The manufacturing carrier gives 2-10 minutes in total at 150-180 °C. They differ widely for thick parts, so cure time is a number to find on test pieces.
Step 6: Open the mold, extract the part and trim the flash.
Worked Example: An 80 × 50 × 6 mm Insulating Block
- Volume = 8 cm × 5 cm × 0.6 cm = 24 cm³.
- With an assumed density of 1.35 g/cm³ (a typical filled phenolic, not a corpus figure): 24 × 1.35 = 32.4 g.
- Charge = 32.4 × 1.05 = 34.0 g.
- Projected area = 80 mm × 50 mm = 4,000 mm² = 4 × 10⁻³ m².
- Force at 10 MPa = 10 × 10⁶ × 4 × 10⁻³ = 40,000 N = 40 kN; at 30 MPa = 120 kN. That is about 4 to 12 tonnes-force.
- Hold time for a 6 mm part: 6 × 1 = 6 min up to 6 × 5 = 30 min by the scratch carrier, against 2-10 min by the other. Find the right value from test pieces.
For comparison, the corpus’s hydraulic press produces 157 kN from a 100 mm ram at 20 MPa, so this part is well within reach of such a press.
Reading The Result
- Short, unfilled corners: too little charge, or mold too cold.
- Thick flash: too much charge, or worn mold faces.
- Blisters or swelling when ejected: gas not vented, or cured too fast; the standard remedy is to open the press briefly early in the cycle to let gas out (general knowledge).
- Soft, tacky part: undercured.
- Part sticks: no draft, rough mold surface or no release agent.
Common Mistakes
- Cold mold — the powder does not flow before it cures.
- Overfilling heavily.
- Opening the press before the cure is done.
- Reaching into a hot mold without tongs.
Hot press, crush and fume
The mold at 160-180 °C burns instantly, and a press at 40-120 kN crushes. Keep hands out when the press closes, use tongs, and wear eye protection. Curing phenolic gives off phenol, formaldehyde and, from hexa, ammonia (general knowledge): work outdoors or with strong ventilation.
What’s Next
- Learn next: Machining Plastics — finishing the part
- Combine with: Electrical Insulation — what the part is for